This course is designed for experimental basic training, it covers basic theoretical knowledge of analytical chemistry as well as common analytical instruments. (Calibration of Analysis Glassware, Calibration of Electrical Conductibility, pH Meter and Sample Determination. Potentiometric Titration of HCl and HAc Mixtures, Redox titration and Determination of Aluminum in Gastropin Tablets. These three titration experiments allow students to master basic titration operations and sample pretreatment methods. Colorimetric Fe Analysis, Fluorescence Spectrophotometric Analysis, Redox K3Fe(CN)6 on Glassy Carbon (GC) Electrode, Chemiluminescence Analysis and Detection, Determination of Ascorbic Acid in Vitamin C Tablets by Differential Pulse Voltammetry, UV-vis Spectrum Analysis and Quantitative Determination of Amino Acids, Infrared Spectrometry Unknown organic Compound. At the end of the period, the experimental operation assessment will be carried out. Through one semester of experimental training, after the 12 independent analysis and experimental operation training, the basic experimental operation of the students will be tested in the experimental operation.). Through the study of analysis chemistry experiment courses, the students’ experimental ability is exercised, and the students’ experimental skills and basic qualities of scientific research are cultivated.