This experimental course is aimed at the junior students. A series of basic experiments are set up, involving information materials, energy materials, biomedical materials, advanced processing and manufacturing of materials, as well as the application of these materials and technologies in information, energy, biomedical, aerospace and other fields. Through both professional and interesting experiments, the basic experimental operation skills of students are cultivated, and the understanding of basic theory courses is improved. If the content of the experiment is properly expanded, it can be combined with the college scientific and technological activities and lay a foundation for students to carry out extracurricular scientific and technological innovation activities. At the same time, students will have a preliminary understanding of the connotation of materials discipline and the characteristics of related disciplines, to help students major selection.